Heidolph Hei-VAP Advantage Manuale Utente

Hei-VAP Value Hei-VAP Advantage Operating Instructions

About this Document 2 Hei-VAP Value, Hei-VAP Advantage EN EN 1.2.2 Icons and symbols Warnings The following symbols and signal words will be cont

About this Document Hei-VAP Value, Hei-VAP Advantage 3 EN The following specific safety icons in correspondence with BGV A8 regulations will be

About this Document 4 Hei-VAP Value, Hei-VAP Advantage EN EN Prohibitory signs Icon Explanation Icon Explanation Fire, open flame and smoking

Basic safety instructions Hei-VAP Value, Hei-VAP Advantage 5 EN 2 Basic safety instructions The rotary evaporator is constructed according to c

Basic safety instructions 6 Hei-VAP Value, Hei-VAP Advantage EN EN 2.4 Use in explosion-prone areas Do not use the equipment in explosion-p

Basic safety instructions Hei-VAP Value, Hei-VAP Advantage 7 EN 2.7 Qualifications of Personnel The target group of the rotary evaporator is qu

Basic safety instructions 8 Hei-VAP Value, Hei-VAP Advantage EN EN 2.10 Signs on the equipment Sign Designation Hot surface Risk of entanglemen

Basic safety instructions Hei-VAP Value, Hei-VAP Advantage 9 EN WARNING Hot surfaces! Scalding and burns.  Let the heating bath and glass d

Basic safety instructions 10 Hei-VAP Value, Hei-VAP Advantage EN EN WARNING Imploding glass devices! Serious injuries from shattering glass.

Unit Description Hei-VAP Value, Hei-VAP Advantage 11 EN 3 Unit Description Rotary evaporators Hei-VAP Value, Hei-VAP Advantage, Hei-VAP Precisi

Set-up and Start-up 12 Hei-VAP Value, Hei-VAP Advantage EN EN EN 4 Set-up and Start-up 4.1 Scope of delivery Descrip-tion Completion Quanti

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 13 EN Included with the equipment: Description Quantity Order number Vapor tube couplin

Set-up and Start-up 14 Hei-VAP Value, Hei-VAP Advantage EN EN 4.2 Transport The motor lift units have a transportation safety device, which must

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 15 EN 4. Switch off the unit. 5. Remove the plug. 6. Package the unit. CAUTION Vibr

Set-up and Start-up 16 Hei-VAP Value, Hei-VAP Advantage EN EN 1. Place the base plate (2) on the surface for the heating bath (1) into the provi

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 17 EN Location of the heating bath when using Rotacool  The base unit is located on a

Set-up and Start-up 18 Hei-VAP Value, Hei-VAP Advantage EN EN In order to operate the equipment in a country with a different connector system, o

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 19 EN 4.4.6 Operating the lift In order to be able to control the immersion depth of the

Set-up and Start-up 20 Hei-VAP Value, Hei-VAP Advantage EN EN WARNING Glass breakage! Serious injuries from shattering and breaking glass. 

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 21 EN WARNING Risk of injuries due to retracting or entrapment! Risk of injury. A risk

Translation of the original operating instructions. The operating instructions must be read prior to the initial star

Set-up and Start-up 22 Hei-VAP Value, Hei-VAP Advantage EN EN 1. Remove the vapor tube from the packaging. Figure 4–7: Install the vapor tube

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 23 EN Figure 4–9: Placing the PTFE 26 vacuum on the vapor tube 1 PTFE 26 vacuum seal 2 V

Set-up and Start-up 24 Hei-VAP Value, Hei-VAP Advantage EN EN WARNING Risk of injuries due to retracting or entrapment! Risk of injury. A risk

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 25 EN  Push the threaded connection (2) over the condenser flange.  Push the spring

Set-up and Start-up 26 Hei-VAP Value, Hei-VAP Advantage EN EN 4.5.5 Install the evaporator flask WARNING Glass breakage! Serious injuries fr

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 27 EN 4.5.6 Setting the evaporator flask inclination The inclination of the evaporator f

Set-up and Start-up 28 Hei-VAP Value, Hei-VAP Advantage EN EN 4.5.7 Setting the immersion depth of the evaporator flask CAUTION Unintentionall

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 29 EN 4.5.8 Release the evaporator flask from the vapor tube WARNING Glass breakage! S

Set-up and Start-up 30 Hei-VAP Value, Hei-VAP Advantage EN EN 4.5.9 Insert the inlet tube The inlet tube consists of:  Stopcock (Stopper) 

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 31 EN 4.5.11 Assemble the collecting flask 1. Hold the receiving flask with the ball-

Set-up and Start-up 32 Hei-VAP Value, Hei-VAP Advantage EN EN 4.5.13 Connect the vacuum The Woulff flask is connected to the vacuum valve (excep

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 33 EN 1. Unscrew the threaded fitting (4) from the Woulff bottle, remove the hose clamp

Set-up and Start-up 34 Hei-VAP Value, Hei-VAP Advantage EN EN Figure 4–20: Hei-VAP Advantage with Rotavac valve control and Vac control automati

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 35 EN Figure 4–22: Hei-VAP Precision with Rotavac valve control and vacuum box 1 Condens

Set-up and Start-up 36 Hei-VAP Value, Hei-VAP Advantage EN EN Figure 4–24: Hei-VAP Precision with Rotavac vario tec and vacuum box 1 Condenser 7

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 37 EN 4.6 Feed the distilled material Additional distillation material can be supplied

Set-up and Start-up 38 Hei-VAP Value, Hei-VAP Advantage EN EN 4.8 Assemble / connect accessories Figure 4–27: Assemble the protective cover 1 H

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 39 EN When using the cover and the protective shield, take care that the two parts do n

Set-up and Start-up 40 Hei-VAP Value, Hei-VAP Advantage EN EN 4.9 Operating the control panel Figure 4–31: Control panel (for Hei-VAP Precision

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 41 EN 2. The cable reel is surrounded by a shell. 3. Pull the control panel apart, so

Table of contents EN Table of contents 1 About this Document ...

Set-up and Start-up 42 Hei-VAP Value, Hei-VAP Advantage EN EN The shell can be turned by 180° as desired, in order to adjust the surface and view

Set-up and Start-up Hei-VAP Value, Hei-VAP Advantage 43 EN Figure 4–32: Vacuum box (for Hei-VAP Precision) 1 USB PC connection 2 Vacuum pum

Switching on the base unit 44 Hei-VAP Value, Hei-VAP Advantage EN EN 5 Switching on the base unit 1. Switch on the base unit by pressing the to

Operation of the Hei-VAP Value Hei-VAP Value, Hei-VAP Advantage 45 EN 6 Operation of the Hei-VAP Value The basic steps of operating the rotar

Operation of the Hei-VAP Value 46 Hei-VAP Value, Hei-VAP Advantage EN EN 6.2 Setting the heating bath temperature  The control dial for the he

Operation of the Hei-VAP Advantage Hei-VAP Value, Hei-VAP Advantage 47 EN 7 Operation of the Hei-VAP Advantage The basic steps of operating t

Operation of the Hei-VAP Advantage 48 Hei-VAP Value, Hei-VAP Advantage EN EN 7.1 Setting the heating bath temperature  The heating bath is fil

Operation of the Hei-VAP Advantage Hei-VAP Value, Hei-VAP Advantage 49 EN The last set medium will be taken over after 10 seconds of inactivit

Operation of the Hei-VAP Advantage 50 Hei-VAP Value, Hei-VAP Advantage EN EN  The unit is switched on.  The rotary evaporator is operational

Operation of the Hei-VAP Advantage Hei-VAP Value, Hei-VAP Advantage 51 EN 7.4 Timing functions 7.4.1 Timer The timer function stops the dist

Table of contents 6 EN 4.6 Feed the distilled material ...

Errors and Troubleshooting 52 Hei-VAP Value, Hei-VAP Advantage EN EN EN 8 Errors and Troubleshooting 8.1 General errors Error / message

Errors and Troubleshooting Hei-VAP Value, Hei-VAP Advantage 53 EN Error / message Cause Remedy No evacuation Power switch Rotavac vario control

Errors and Troubleshooting 54 Hei-VAP Value, Hei-VAP Advantage EN EN EN 8.3 Hei-VAP Value Error / message (flashing code) Cause Remedy **

Errors and Troubleshooting Hei-VAP Value, Hei-VAP Advantage 55 EN 8.4 Hei-VAP Advantage Error / message (error label) Cause Remedy 1 The transp

Errors and Troubleshooting 56 Hei-VAP Value, Hei-VAP Advantage EN EN EN The rotary evaporator is checked after "power on" in an

Maintenance, cleaning, service Hei-VAP Value, Hei-VAP Advantage 57 EN 9 Maintenance, cleaning, service 9.1 Maintenance  Only use genuine par

Maintenance, cleaning, service 58 Hei-VAP Value, Hei-VAP Advantage EN EN 9.1.2 Evacuate the heating bath WARNING Verify that the basic device i

Maintenance, cleaning, service Hei-VAP Value, Hei-VAP Advantage 59 EN 1. Screw the valve into the G6 center piece (2) up to the stop. 2. Tur

Maintenance, cleaning, service 60 Hei-VAP Value, Hei-VAP Advantage EN EN 9.3 Cleaning CAUTION Damages due to corrosive cleaning agents! Damage

Dismantling, storage, disposal Hei-VAP Value, Hei-VAP Advantage 61 EN 10 Dismantling, storage, disposal 10.1 Disassembly CAUTION Unintentional

Table of contents EN 12 Appendix ...

Dismantling, storage, disposal 62 Hei-VAP Value, Hei-VAP Advantage EN EN 10.1.2 Disconnecting the coolant / vacuum 1. Verify that the coolant a

Accessories, spare parts Hei-VAP Value, Hei-VAP Advantage 63 EN 11 Accessories, spare parts 11.1 Glass devices Figure 11–1: Glassware set G1

Accessories, spare parts 64 Hei-VAP Value, Hei-VAP Advantage EN EN Figure 11–2: Glassware set G3 Order description Position Order No. Piece

Accessories, spare parts Hei-VAP Value, Hei-VAP Advantage 65 EN Figure 11–3: Glassware set G5 Order description Position Order No. Piece at de

Accessories, spare parts 66 Hei-VAP Value, Hei-VAP Advantage EN EN Figure 11–4: Glassware set G6 Order description Position Order No. Piece a

Accessories, spare parts Hei-VAP Value, Hei-VAP Advantage 67 EN Condenser G6B, plastic coated 17 514-23000-02 (1) Condenser mounting 569-00050-

Appendix 68 Hei-VAP Value, Hei-VAP Advantage EN EN 12 Appendix 12.1 Technical data Basic Device Basis Hei-VAP Value Basis Hei-VAP HL. Basis H

Appendix Hei-VAP Value, Hei-VAP Advantage 69 EN Degree of protection IP 20 Airborne sound level Clearly lower than 85 db(A) Permissible ambient

Appendix 70 Hei-VAP Value, Hei-VAP Advantage EN EN Hei-VAP Precision:  Rotary evaporator Hei-VAP with valve-controlled vacuum pump  Vacuum

Appendix Hei-VAP Value, Hei-VAP Advantage 71 EN 12.3 Solvent data The graph shows the relationship between the pressure and boiling temperature

Appendix 72 Hei-VAP Value, Hei-VAP Advantage EN EN Solvents Total formula MW [g/mol] Boiling point [°C] Δhvap [J/g] Vacuum for a boiling point

Appendix Hei-VAP Value, Hei-VAP Advantage 73 EN 12.4 EC Declaration of Conformity We, Heidolph Instruments GmbH & Co. KG, Heidolph Instrum

Appendix 74 Hei-VAP Value, Hei-VAP Advantage EN EN 12.5 Warranty Statement Heidolph Instruments guarantees a warranty of three years

Appendix Hei-VAP Value, Hei-VAP Advantage 75 EN 12.6 Declaration of non-objection Copy and mail / fax this declaration in the event of repairs

EN 01-005-004-79 05/10/2011 © Heidolph Instruments GmbH & Co. KG Technische Ände

About this Document Hei-VAP Value, Hei-VAP Advantage 1 EN 1 About this Document 1.1 Versions references Version Modification 1.0 07/2009 1.2